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Laboratory 1: Synthesis and Physicochemical Characterization of Inorganic Materials
1.1: Solid-state synthesis
Laboratory:
Laboratory 1: Synthesis and Physicochemical Characterization of Inorganic Materials
Laboratory 1: Synthesis and Physicochemical Characterization of Inorganic Materials
Equipment:
L1.1.1. Planetary Ball Mill 4 × 500ML, Micromolding Solutions Inc./MicroNano Tools, 2016
L1.1.2. High-temperature furnace LHTC (T)08/16 - Nabertherm, 2020
1.2: Hydrothermal synthesis
Laboratory:
Laboratory 1: Synthesis and Physicochemical Characterization of Inorganic Materials
Laboratory 1: Synthesis and Physicochemical Characterization of Inorganic Materials
Equipment:
L1.2.1. Autoclave for hydrothermal synthesis, 300 °С, 150 atm, AIBOTE, 2014
1.3: Sample analysis by X-ray diffraction (XRD)
Laboratory:
Laboratory 1: Synthesis and Physicochemical Characterization of Inorganic Materials
Laboratory 1: Synthesis and Physicochemical Characterization of Inorganic Materials
Equipment:
L1.3.1. X-ray diffractometer APD-15, PHILIPS, 1982
1.4: Sample analysis by scanning electron microscopy (SЕМ)
Laboratory:
Laboratory 1: Synthesis and Physicochemical Characterization of Inorganic Materials
Laboratory 1: Synthesis and Physicochemical Characterization of Inorganic Materials
Equipment:
L1.4.1. Scanning electron microscope, EVO10, 2021
1.5: Determination of specific surface area by the Brunauer-Emmett-Teller (BET) method and pore size distribution of micro- and mesopores
Laboratory:
Laboratory 1: Synthesis and Physicochemical Characterization of Inorganic Materials
Laboratory 1: Synthesis and Physicochemical Characterization of Inorganic Materials
Equipment:
L1.5.1. BET surface area analyzer, STROHLEINE, 1980