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Laboratory 6: Electrode Materials for Batteries and Supercapacitors
6.1: Solid-State Synthesis of Electrode Materials and/or Solid Electrolytes
Laboratory 6: Electrode Materials for Batteries and Supercapacitors
L6.1.1. Ball mills Fritsch Pulverisette 6 (700 rpm) and Fritsch Pulverisette 7 (1100 rpm) 1996
L6.1.2. Rotational Vacuum Evaporator, equipped with Vacuum Controller and Vacuum Pump, R-300, Büchi, 2020
L6.1.3. Thermo-programmable furnaces, Nabertherm, 1000 °C, 2 бр. (муфелна и тръбна), 2009
L6.1.4. Vacuum dryer, equipped with vacuum pump and controller, 2020.
6.2: Synthesis of electrode materials from liquid precursors
Laboratory 6: Electrode Materials for Batteries and Supercapacitors
L6.2.1. Lyophilizer Alfa-Crist, 1996
6.3: X-ray structural qualitative and quantitative phase analysis, determination of crystallite size, microstrain and crystal structure
Laboratory 6: Electrode Materials for Batteries and Supercapacitors
L6.3.1. Powder X-ray Diffractometer Bruker D8 Advance with LynxEye Detector, 2006.
6.4: Analysis of samples with transmission electron microscopy (TEM)
Laboratory 6: Electrode Materials for Batteries and Supercapacitors
L6.4.1. High-resolution transmission electron microscope HRTEM JEOL JEM 2100, equipped with a CCD camera GATAN, 2009
6.5: Thermal analysis
Laboratory 6: Electrode Materials for Batteries and Supercapacitors
L6.5.1. Equip. for diff. thermal & thermograv. analysis and qual. analysis of gases evolved during heating. Qual. analysis of indiv. gases from tested samples: TG/DTA/MASS Seteram Labsys Evo-1600, comb. w/ Quadrupole Mass Spectrometer Pfeiffer, 2009
6.6: Analysis of samples with X-ray photoelectron spectroscopy: qualitative and quantitative analysis
Laboratory 6: Electrode Materials for Batteries and Supercapacitors
L6.6.1. X-ray photoelectron spectroscopy spectrometer, AXIS SUPRA Kratos Analytical LTd.
6.7: Analysis of samples with electron paramagnetic resonance spectroscopy
Laboratory 6: Electrode Materials for Batteries and Supercapacitors
L6.7.1. Electron paramagnetic resonance spectrometer, BRUKR EMX+, 2014
6.8: Analysis of samples with infrared spectroscopy (IR)
Laboratory 6: Electrode Materials for Batteries and Supercapacitors
L6.8.1. Infrared spectrometer, NICOLET iS5 FTIR
6.9: Measurement of electrical conductivity of solid samples over a wide temperature range
Laboratory 6: Electrode Materials for Batteries and Supercapacitors
L6.9.1. Equipment for measuring electrical conductivity of materials over a wide temperature range MMR system K2500-SLP-SP, 2010 г.
6.10: Measurement of thermal conductivity
Laboratory 6: Electrode Materials for Batteries and Supercapacitors
L6.10.1. Thermal conductivity and effusivity measuring equipment C-Therm TCiTM